Synthesis process ea tantalum pentachloride

Mokhoa oa ho kopanya oatantalum pentachloridehaholo-holo e kenyelletsa mehato e latelang:

1, Tokiso ea thepa e tala

Lokisetsa bohloeki bo phahamengtšepe ea tantalumle chlorine e phahameng-hloeka kapa hydrogen chloride (HCl) e le lisebelisoa tse tala. Bohloeki batantalumtšepee na le tšusumetso e kholo ho hloekeng ha sehlahisoa sa ho qetela.

2. Karabelo ea chlorination

Mokhoa o tobileng oa chlorination: tšepe ea Tantalum e khangoa kapa e phofshoa, ebe e kenngoa ka har'a khase ea chlorine bakeng sa karabelo ea chlorination sebakeng sa mocheso oa 170-250. Khase ea chlorine e kopana le tantalum ho hlahisa tantalum pentachloride. Karabelo ena e ka boela ea etsoa ho sebelisoa HCl, empa e hloka ho etsoa ka mocheso o phahameng (joalo ka 400).

Mokhoa o sa tobang oa chlorination: Tantalum pentachloride e ka boela ea fumanoa ka ho arabela tantalum pentoxide ka thionyl chloride (SOCl2) ho 240 ° C. Equation ea reaction ke:

Ta2O5+5 SOCl2 → 2 TaCl5+5 SO2.

3、 Karohano le tlhoekiso

Folisa khase e hlahisoang ke chlorination reaction ho e kopanya hore e be mokelikeli.

Arola le ho hloekisa metsi a tantalum pentachloride ho litšila. Hangata, li-distillation le mekhoa e meng li sebelisoa ho arola litšila tse fapaneng ho latela phapang ea tsona ea ntlha e belang. Mohato ona ke senotlolo sa ho netefatsa bohloeki ba tantalum pentachloride.

4、 Ho omisa kalafo

Omisa tse arohaneng le tse hloekisitsoengtantalum pentachlorideho tlosa mongobo o ka hodimo le ditshila. Ho omisa kalafo ho bohlokoa bakeng sa ho boloka botsitso le bohloeki ba tantalum pentachloride.

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Nako ea poso: Sep-05-2024